By Tatsuki Ohji, Mrityunjay Singh
This ebook is a set of papers from the yank Ceramic Society's thirty fifth overseas convention on complicated Ceramics and Composites, held in Daytona seashore, Florida, January 23-28, 2011. This factor contains papers provided within the fifth foreign Symposium on complex Processing and production applied sciences for Structural and Multifunctional fabrics and structures on themes comparable to Design-Oriented production and Novel Forming and Sintering. Papers from a unique consultation held in honor of Katsutoshi Komeya of Yokohama nationwide collage, Japan also are included.Content:
Read or Download Advanced Processing and Manufacturing Technologies for Structural and Multifunctional Materials V: Ceramic Engineering and Science Proceedings, Volume 32 PDF
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Extra info for Advanced Processing and Manufacturing Technologies for Structural and Multifunctional Materials V: Ceramic Engineering and Science Proceedings, Volume 32
A droplet experiment at ~ 200 μπι/s, however, resulted in an isotropic microstructure. Figure 7A gives an overview of the complete experimental results. The transition velocity from a lamellar microstructure to an isotropic microstructure is drastically shifted to smaller solidification velocities with increasing particle sizes. Figure 7. 8 μπιΐο 15 μπι. 6 μκι for solidification velocities below and above the critical solidification velocity. 4 DISCUSSION AND CONCLUSIONS The main objective of the experiments was to identify the microstructure morphologies, which can be created by directional solidification of water based particle suspensions and to determine the critical processing conditions for morphology transitions.
8 μπι, cooling plate temperature -10 °C. Most important results are summarized in Fig. 5; detailed data and a quantitative analysis of the complete data set are subject of a forthcoming paper. The measurements show, that the empirical dependence of the lamellae spacmg λ on the solidification velocity v can be described by a power law (\ a v'1), as already reported by Deville et alA The influence of particle size on the lamellae Advanced Processing and Manufacturing Technologies for Structural and Multifunctional Materials V ■ 39 Microstructure Maps for Unidirectional Freezing of Particle Suspensions development is not clearly identified in literature.
2 μιη particle suspensions, all systems undergo a change from lamellar to isotropic, when a critical solidification velocity is exceeded (Figure 7B). 1 μηι, the microstructure is lamellar for solidification velocities of 8 and 10 μπι/s, respectively, but isotropic for 20 μπι/s. 6 μπι, the microstructure transition occurs by changing the solidification velocity from 5 to 8 μιη/s. The 15 μιη particle suspensions form lamellae at 1 μηι/s, but are entrapped at 8 μηι/s. 2 μπι particle suspension solidifies to a lamellar microstructure up to 10 μιη/s.